D. Basrur; J. Ishwara Bhat
Abstract
In this work, the preparation of activated carbons from agricultural product, the fenugreek seeds by two approaches, chemical and microwave activation methods were studied. The characterization of carbon materials were carried out using different techniques such as Fourier Transform ...
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In this work, the preparation of activated carbons from agricultural product, the fenugreek seeds by two approaches, chemical and microwave activation methods were studied. The characterization of carbon materials were carried out using different techniques such as Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), Thermo Gravimetric Analysis (TGA), X-Ray Diffraction (XRD). Adsorption experiment was carried out for the adsorption of two different basic dyes, Methylene Blue (MB) and Crystal Violet (CV) under varying conditions such as concentration, agitation time and temperature. The data acquired from concentration variation were found to fit well with Langmuir and also Freundlich isotherms. Kinetic studies revealed the fact that the system followed second order adsorption rate. Thermodynamic parameters such as ΔH≠, ΔS≠ and ΔG≠ were calculated from the obtained data on adsorption at different temperature.
D. Basrur; J. Ishwara Bhat
Abstract
In this study the preparation of activated carbon from agricultural product were reported. The fenugreek seeds were activated by chemical and microwave activation methods. The characterization of carbon materials were carried out using different techniques like Fourier Transform Infrared Spectroscopy ...
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In this study the preparation of activated carbon from agricultural product were reported. The fenugreek seeds were activated by chemical and microwave activation methods. The characterization of carbon materials were carried out using different techniques like Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), Thermo Gravimetric Analysis (TGA), X-Ray Diffraction (XRD). Adsorption experiment was carried out for the adsorption of two different basic dyes, Methylene Blue (MB) and Crystal Violet (CV) under varying conditions such as concentration of dye, mixing time and adsorption temperature. The data acquired from concentration variation were found to fit well with Langmuir and also Freundlich isotherms. Kinetic studies revealed the fact that the system follows second order. Thermodynamic parameters like ΔH≠, ΔS≠ and ΔG≠ were calculated from the study on adsorption at different temperature. The adsorbent preparation via microwave technology is a desired methods which is resulted in conservation of energy for an efficient production of activated carbon.